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Registro Completo |
Biblioteca(s): |
Embrapa Florestas. |
Data corrente: |
10/12/2014 |
Data da última atualização: |
18/02/2015 |
Tipo da produção científica: |
Artigo em Periódico Indexado |
Autoria: |
WELKE, J. E.; ZANUS, M. C.; LAZZAROTTO, M.; PULGATI, F. H.; ZINI, C. A. |
Afiliação: |
JULIANE ELISA WELKE, UFRGS; MAURO CELSO ZANUS, CNPUV; MARCELO LAZZAROTTO, CNPF; FERNANDO HEPP PULGATI, UFRGS; CLÁUDIA ALCARAZ ZINI, UFRGS. |
Título: |
Main differences between volatiles of sparkling and base wines accessed through comprehensive two dimensional gas chromatography with time-of-flight mass spectrometric detection and chemometric tools. |
Ano de publicação: |
2014 |
Fonte/Imprenta: |
Food Chemistry, v. 164, p. 427-437, 2014. |
Idioma: |
Inglês |
Conteúdo: |
The main changes in the volatile profile of base wines and their corresponding sparkling wines produced by traditional method were evaluated and investigated for the first time using headspace solid-phase microextraction combined with comprehensive two-dimensional gas chromatography with timeof- flight mass spectrometry detection (GC GC/TOFMS) and chemometric tools. Fisher ratios helped to find the 119 analytes that were responsible for the main differences between base and sparkling wines and principal component analysis explained 93.1% of the total variance related to the selected 78 compounds. It was also possible to observe five subclusters in base wines and four subclusters in sparkling wines samples through hierarchical cluster analysis, which seemed to have an organised distribution according to the regions where the wines came from. Twenty of the most important volatile compounds co-eluted with other components and separation of some of them was possible due to GC GC/TOFMS performance. |
Palavras-Chave: |
Composto volátil. |
Thesagro: |
Vinho. |
Categoria do assunto: |
-- |
Marc: |
LEADER 01670naa a2200193 a 4500 001 2002075 005 2015-02-18 008 2014 bl uuuu u00u1 u #d 100 1 $aWELKE, J. E. 245 $aMain differences between volatiles of sparkling and base wines accessed through comprehensive two dimensional gas chromatography with time-of-flight mass spectrometric detection and chemometric tools.$h[electronic resource] 260 $c2014 520 $aThe main changes in the volatile profile of base wines and their corresponding sparkling wines produced by traditional method were evaluated and investigated for the first time using headspace solid-phase microextraction combined with comprehensive two-dimensional gas chromatography with timeof- flight mass spectrometry detection (GC GC/TOFMS) and chemometric tools. Fisher ratios helped to find the 119 analytes that were responsible for the main differences between base and sparkling wines and principal component analysis explained 93.1% of the total variance related to the selected 78 compounds. It was also possible to observe five subclusters in base wines and four subclusters in sparkling wines samples through hierarchical cluster analysis, which seemed to have an organised distribution according to the regions where the wines came from. Twenty of the most important volatile compounds co-eluted with other components and separation of some of them was possible due to GC GC/TOFMS performance. 650 $aVinho 653 $aComposto volátil 700 1 $aZANUS, M. C. 700 1 $aLAZZAROTTO, M. 700 1 $aPULGATI, F. H. 700 1 $aZINI, C. A. 773 $tFood Chemistry$gv. 164, p. 427-437, 2014.
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Embrapa Florestas (CNPF) |
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Registro Completo
Biblioteca(s): |
Embrapa Semiárido; Embrapa Uva e Vinho. |
Data corrente: |
06/10/2017 |
Data da última atualização: |
23/05/2019 |
Tipo da produção científica: |
Artigo em Periódico Indexado |
Circulação/Nível: |
A - 1 |
Autoria: |
NICOLLI, K. P.; BIASOTO, A. C. T.; SOUZA-SILVA, E. A.; GUERRA, C. C.; SANTOS, H. P. dos; WELKE, J. E.; ZINI, C. A. |
Afiliação: |
Karine P. Nicolli, Institute ofChemistry,UniversidadeFederaldoRioGrandedoSul(UFRGS),91501970PortoAlegre,RS,Brazil; ALINE TELLES BIASOTO MARQUES, CPATSA; Érica A. Souza-Silva, Chemistry Department,UniversidadeFederaldeSão Paulo(UNIFESP),09972-270Diadema,Brazil; CELITO CRIVELLARO GUERRA, CNPUV; HENRIQUE PESSOA DOS SANTOS, CNPUV; JulianeE.Welke, Institute ofFoodScienceandTechnology,UFRGS,91501970PortoAlegre,RS,Brazil; Cláudia A.Zini, Institute ofChemistry,UniversidadeFederaldoRioGrandedoSul(UFRGS),91501970PortoAlegre,RS,Brazil. |
Título: |
Sensory, olfactometry and comprehensive two-dimension algas chromatography analyses as appropriate tools to characterize the effects of vine management on wine aroma |
Ano de publicação: |
2018 |
Fonte/Imprenta: |
Food Chemistry, v. 243, p. 103-117, 2018. [online] |
Idioma: |
Inglês |
Conteúdo: |
For the first time, the in fluence of different vine management was evaluated in relation to volatile profile and sensory perception through GC × GC/TOFMS, QDA, GC-FID, GC/MS, and GC-O. GC × GC/TOFMS analyses and QDA have shown that a larger spacing between vine rows (2 rather than 1 m), attachment of shoots upwards, and irrigation did not result in wine improvement. Conversely, wines elaborated with grapes from a vine with a lower bud load (20 per plant; sample M1) stood out among the other procedures, rendering the most promising wine aroma. GC × GC/TOFMS allowed identification of 220 compounds including 26 aroma active compounds also distinguished by GC-O. Among them, eight volatiles were important to differentiate M1 from other wines, and five out of those eight compounds could only be correctly identified and quantified after separation in second dimension. Higher levels of three volatiles may explain the relation of M1 wine with red and dry fruits. |
Palavras-Chave: |
Chromatography analyses; GC-O; HS-SPME-GC × GC/TOFM; HS-SPME-GC ×GC/TOFMS; QDA; Vine management; Wine aroma. |
Thesagro: |
Uva. |
Thesaurus NAL: |
Canopy; Grapes; Volatile compounds. |
Categoria do assunto: |
-- F Plantas e Produtos de Origem Vegetal |
URL: |
https://ainfo.cnptia.embrapa.br/digital/bitstream/item/164739/1/Food-Chemistry-243-2018-103117-Nicolli.pdf
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Marc: |
LEADER 01941naa a2200325 a 4500 001 2076841 005 2019-05-23 008 2018 bl uuuu u00u1 u #d 100 1 $aNICOLLI, K. P. 245 $aSensory, olfactometry and comprehensive two-dimension algas chromatography analyses as appropriate tools to characterize the effects of vine management on wine aroma$h[electronic resource] 260 $c2018 520 $aFor the first time, the in fluence of different vine management was evaluated in relation to volatile profile and sensory perception through GC × GC/TOFMS, QDA, GC-FID, GC/MS, and GC-O. GC × GC/TOFMS analyses and QDA have shown that a larger spacing between vine rows (2 rather than 1 m), attachment of shoots upwards, and irrigation did not result in wine improvement. Conversely, wines elaborated with grapes from a vine with a lower bud load (20 per plant; sample M1) stood out among the other procedures, rendering the most promising wine aroma. GC × GC/TOFMS allowed identification of 220 compounds including 26 aroma active compounds also distinguished by GC-O. Among them, eight volatiles were important to differentiate M1 from other wines, and five out of those eight compounds could only be correctly identified and quantified after separation in second dimension. Higher levels of three volatiles may explain the relation of M1 wine with red and dry fruits. 650 $aCanopy 650 $aGrapes 650 $aVolatile compounds 650 $aUva 653 $aChromatography analyses 653 $aGC-O 653 $aHS-SPME-GC × GC/TOFM 653 $aHS-SPME-GC ×GC/TOFMS 653 $aQDA 653 $aVine management 653 $aWine aroma 700 1 $aBIASOTO, A. C. T. 700 1 $aSOUZA-SILVA, E. A. 700 1 $aGUERRA, C. C. 700 1 $aSANTOS, H. P. dos 700 1 $aWELKE, J. E. 700 1 $aZINI, C. A. 773 $tFood Chemistry$gv. 243, p. 103-117, 2018. [online]
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